FIRST SCHEDULE
Excise Bond Security Form
(r. 19 (4)) |
EXCISE BOND SECURITY FORM |
BOND FOR PROTECTION OF EXCISE DUTIES |
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I/We.................................................................Of (Address).............................................and (Guarantor)..................................of (Address)............................................................ |
Hereby acknowledge that I/we am/are bound to the Commissioner of Domestic Taxes in the sum of .............. ..shillings to be paid to the Commissioner of Domestic Taxes for which payment I/we bind myself/ourselves jointly and severally and also my/our heirs, executors, administrators and assigns and each of them in respect of |
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Dated this ..................................day of................................... , 20.................... |
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WHEREAS the above named....................................................................... has/have been granted a licence to manufacture excisable goods and whereas the above named is/are required to pay the excise duty thereon in accordance with the provisions of the Excise Duty laws not later than the twentieth day of the month next succeeding that in which the duty becomes due or within such other time as may be determined by the Commissioner. |
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Now the condition of this obligation is such that if the above named shall pay the full duties due or charged within that time then this obligation shall be void but otherwise shall be and remain in full force. |
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Signed, sealed and delivered byThe above named......................................... | }} |
In the presence of ..............................(name) | } |
................................................ designation) | } |
of................................................ (address) | } |
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Signed, sealed and delivered byThe above named......................................... | }} |
In the presence of ..............................(name) | } |
................................................ designation) | } |
of................................................ (address) | } |
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Approved | .................................................Commissioner |
SECOND SCHEDULE
SUBSTANCES TO BE MIXED WITH SPIRITS FOR THE PURPOSE OF MANUFACTURING DENATURED SPIRITS
Completely Denatured Spirits (CDS)(i)In the case of completely denatured spirits (CDS-1), to every 90 parts by volume of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added 10 parts by volume of methyl alcohol and one-half of one part by volume of crude pyridine and to each 1000 litres of the mixture of which is added 3.75 litres kerosene petroleum oil and not less than 1.5 grams of powdered methyl violet dye.(ii)In the case if completely denatured spirits (CDS-2) to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added 2 litres of methyl ethyl ketone, 3 litres of methyl isobutyl ketone, 1 gram of denatonium benzoate and not less than 0.2 grams of powdered methylene blue dye.(iii)In the case of completely denatured spirits for export (CDS—E) to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added denaturants in accordance with the regulations prescribed by the Government of a foreign country to which the denatured spirits will be exported.Specially Denatured Spirits (SDS)(iv)In the case of specially denatured spirits (SDS-1) to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added 4 litres of methyl alcohol and not less than 1 gram of denatonium benzoate.(v)In the case of specially denatured spirits (SDS-2), to every to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added 4 litres of methyl alcohol and not less than 250 grams of sucrose octaacetate.(vi)In the case of specially denatured spirits (SDS-3), to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added 3 litres of isopropyl alcohol and not less than 2 grams of denatonium benzoate.(vii)In the case of specially denatured spirits (SDS-4), to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added two and one-half litres of diethyl phthalate and not less than 125 millilitres of tert-butyl alcohol.(viii)In the case of specially denatured spirits (SDS-5), to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added 250 grams of sucrose octaacetate and not less than 100 millilitres of tert-butyl alcohol.(ix)In the case of specially denatured spirits (SDS-6), to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added 1 gram of denatonium benzoate and not less than 100 millilitres of tert-butyl alcohol.(x)In the case of specially denatured spirits for export (SDS—E), to every 100 litres of ethyl alcohol of an alcoholic strength by volume of not less than 94 per cent there shall be added denaturants in accordance with the regulations prescribed by the Government of a foreign country to which the denatured spirits will be exported.Power Alcohol(xi)In the case of power alcohol for use in motor spirit, to every one hundred parts by volume of anhydrous ethanol add one part by volume of motor spirit (gasoline) regular.THIRD SCHEDULE
CONDITIONS TO WHICH DENATURANTS MUST CONFORM
1.Methyl alcohol(i)Methyl alcohol shall be clear colourless liquid and free from matter in suspension, as assessed by visual inspection, and shall consist essentially of methanol, CH3OH.(ii)The density of the material at 20°C shall be not lower than 0.791 g/mL and not higher than 0.794 g/lm.(iii)When the material is distilled, the distillation range at 1013 millibars pressure shall not exceed 1.0°C and shall include the value 64.6°C.(iv)The residue on evaporation of the material shall not exceed 0.001% (m/m).(v)The material shall not be alkaline to phenolphthalein and shall not contain more than 0.003% (m/m) of acid, calculated as formic acid (HCOOH).(vi)The material shall not contain more than 0.005% (m/m) of aldehydes and ketones, calculated as acetone (CH3COCH3).(vii)The material shall not contain more than 0.1% (m/m) of water.(viii)The material shall contain methyl alcohol purity of not less than 99.85% v/v2.Isopropyl alcohol(i)Isopropyl alcohol shall be clear colourless liquid and free from matter in suspension, as assessed by visual inspection, and shall consist essentially of propan-2-ol, (CH3)2CHOH.(ii)The density of the material at 20°C shall be not lower than 0.785 g/mL and not higher than 0.787 g/ml.(iii)When the material is distilled, the initial boiling point at 1013 millibars pressure shall be not lower than 81.5°C and the dry point at 1013 millibars pressure shall be not higher than 83.0°C.(iv)The residue on evaporation of the material shall not exceed 0.002% (m/m).(v)The material shall not contain more than 0.50% (m/m) of water.(vi)The material shall not be alkaline to phenolphthalein and shall not contain more than 0.002 % (m/m) of acid, calculated as acetic acid (CH3COOH).(vii)The material shall not contain more than 0.10 % (m/m) of aldehydes and ketones, calculated as acetone (CH3COCH3).(viii)The material shall contain isopropyl alcohol purity of not less than 95% v/v.3.Tertiary-Butyl alcohol(i)Tertiary-Butyl alcohol shall be clear colorless liquid and free from matter in suspension, as assessed by visual inspection, and shall consist essentially of 2-methyl-2-propanol, (CH3)3COH.(ii)Freezing point (first needle) above 20°C.(iii)Specific gravity at 25°C/25°C. 0.780 to 0.786.(iv)When 100 ml of tertiary butyl alcohol is distilled, none shall distil below 78°C and none above 85°C at 1013 millibars pressure. More than 95 percent shall distil between 81°C and 83°C.(v)Acidity (as acetic acid). 0.003 percent by weight maximum.(vi)Identification test. Place five drops of a solution containing approximately 0.1 percent tertiary butyl alcohol in ethyl alcohol in a test tube. Add 2 ml of Denige's reagent (dissolve 5 grams of red mercuric oxide in 20 ml of concentrated sulphuric acid; add this to 80 mL of distilled water, and filter when cool). Heat the mixture just to the boiling point and remove from the flame. A yellow precipitate forms within a few seconds.(vii)The material shall contain Tertiary-Butyl alcohol purity of not less than 95%v/v.4.Methyl ethyl ketone(i)Methyl ethyl ketone shall be clear colourless liquid and free from matter in suspension, as assessed by visual inspection, and shall consist essentially of 2-butanone (ethyl methyl ketone), CH3COCH2CH3.(ii)The density of the material at 20°C shall be not lower than 0.803 g/mL and not higher than 0.805 g/ml.(iii)When the material is distilled, the initial boiling point at 1013 millibars pressure shall be not lower than 79.0°C and the dry point at 1013 millibars pressure shall be not higher than 81.0°C.(iv)The residue on evaporation of the material shall not exceed 0.002 % (m/m).(v)The material shall not contain more than 0.15% (m/m) of water.(vi)The acidity of the material, calculated as acetic acid (CH3COOH), shall not exceed 0.004 % m/m.(vii)The material shall contain not more than 0.70 % (m/m) of alcoholic impurities, calculated as butanol (C4H9OH).(viii)The material shall contain methyl ethyl ketone purity of not less than 95%v/v.5.Methyl isobutyl ketone(i)Methyl isobutyl ketone shall be clear colourless liquid and free from matter in suspension, as assessed by visual inspection, and shall consist essentially of 4-methylpentan-2-one, CH3COCH2CH (CH3)2.(ii)The density of the material at 20°C shall be, not lower than 0.799 g/mL and not higher than 0.802 g/mL.(iii)When the material is distilled, the initial boiling point at 1013 millibars pressure shall be not lower than 114.0°C and the dry point at 1013 millibars pressure shall be not higher than 117.0°C.(iv)The residue on evaporation of the material shall not exceed 0.002 % (m/m).(v)The material shall contain not more than 0.10% (m/m) of water. The acidity of the material, calculated as acetic acid (CH3COOH).(vi)The material shall contain not more than 0.30% (m/m) of alcoholic impurities, calculated as hexanol (C6H130H).(vii)The material shall contain methyl isobutyl ketone purity of not less than 95% v/v.6.Sucrose octaacetate(i)Sucrose octaacetate shall be white or cream-coloured powder, as assessed by visual inspection, and shall consist essentially of sucrose octaacetate, C28H38O19.(ii)Melting point not less than 78.0°C.(iii)Free acid (as acetic acid). Maximum percentage 0.15 by weight when determined by the following procedure: Dissolve 1.0 gram of sample in 50 ml of neutralized ethyl alcohol and titrate with 0.1N sodium hydroxide using phenolphthalein indicator.Percent acid as acetic acid = ml NaOH used x 0.6/weight of sample.(iv)Purity. Sucrose octaacetate 98 percent minimum by weight, when determined by the following procedure: Transfer a weighed 1.50 grams sample to a 500 ml Erlenmeyer flask containing 100 ml of neutral ethyl alcohol and 50.0 ml of 0.5 N sodium hydroxide. Reflux for 1 hour on a steam bath, cool and titrate the excess sodium hydroxide with 0.5 N sulphuric acid using phenolphthalein indicator.Percent sucrose octaacetate = (ml NaOH — ml H2SO4) x 4.2412/weight of sample7.Diethyl phthalate(i)Diethyl phthalate shall be clear colourless liquid as assessed by visual inspection, and shall consist essentially of ethyl benzene-1, 2-dicarboxylate, c- C12H14O4.(ii)Specific gravity at 25°C/25°C. 1.115 to 1.118.(iii)Refractive index at 25°C. 1.497 to 1.502.(iv)Ester content (as diethyl phthalate). Not less than 99 percent by weight.Note. The sample taken for ester determination should be approximately 0.8 gram.The number of ml of 0.5 N potassium hydroxide used in saponification multiplied by 0.05555 indicates the number of grams of ester in the sample taken for assay.8.Denatonium benzoate(i)Denatonium benzoate shall be white powder as assessed by visual inspection, and shall consist essentially of benzyldiethyl [(2, 6-xylylcarbamoyl) methyl] ammonium benzoate, C28H34N203.(ii)Melting point: Not less than 163°C and not more than 170°C, on a dried specimen.(a)Dissolve about 150 mg in 10 ml of water, and add 15 ml of trinitrophenol: a yellow precipitate is formed.(b)Dissolve about 100 mg in 10 mL of water, and add 20 mL of 2N sulphuric acid and 15 mL of ammonium reineckate (shake about 500 mg of ammonium reineckate with 20 mL of water frequently during 1 hour, and filter. Use within 2 days). Mix, filter through a sintered-glass crucible using gentle suction, and wash thoroughly with water. Remove as much water as possible with suction, and then dry in an oven at 105°C for 1 hour: the denatonium reineckate so obtained melts at about 170°C.(iv)Assay. Contains not less than 99 percent by weight benzyldiethyl [(2,6-xylylcarbamoyl) methyl] ammonium benzoate when assayed by the following method: Dissolve about 900 mg of denatonium benzoate, previously dried and accurately weighed, in 50 ml of glacial acetic acid, add 1 drop of crystal violet (dissolve 100 mg of crystal violet in 10 mL of glacial acetic acid), and titrate with 0.1N perchloric acid to a green end-point. Perform a blank determination, and make any necessary correction. Each mL of 0.1N perchloric acid is equivalent to 44.66 mg of denatonium benzoate, C28H34N203.9.Crude Pyridine(i)Crude pyridine must consist of pyridine bases and must not be more deeply coloured than a mixture of 2 millilitres of 0.05 molar iodine with one litre of water.(ii)It must mix readily and completely with alcohol of a strength of not less than 95 per cent alcohol by volume and must give a clear or only slightly opalescent solution when mixed with twice its volume of water.(iii)10 millilitres of a 1 per cent solution in water must produce immediately a distinct crystalline precipitate on vigorous shaking after the addition of 5 millilitres of an aqueous solution of cadmium chloride containing 5 grammes of the anhydrous fused salt in 100 millilitres, and produce an abundant separation of crystals within 10 minutes.(iv)A white precipitate must be formed when 10 millilitres of a 1 per cent solution in water are mixed with 5 millilitres of Nessler's reagent.(v)1 millilitre of crude pyridine dissolved in 10 millilitres of distilled water must require not less than 9.5 millilitres of 0.5 molar sulphuric acid for neutralisation using screened methyl orange as an indicator.(vi)100 millilitres distilled in accordance with Determination of distillation characteristics of volatile organic liquids (IP 195/98(2004)) (BS 2000-195:1998) must give a distillate of at least 50 millilitres at a temperature of 140°C and of 90 millilitres at 160°C.10.Kerosene petroleum oilKerosene petroleum oil (mineral naphtha) must be of a specific gravity of not less than 0.800 at a temperature of 15.5°C and must possess the characteristic odour and taste of commercial paraffin oil used for burning purposes.11.Methyl violet (Crystal violet) dye (Colour Index No.42555)(i)Methyl violet dye (methylrosaniline chloride, C25H30N3C1) must be in the form of small crystals readily and completely soluble in alcohol of strength of not less than 95 per cent alcohol by volume.(ii)Identification test. Sprinkle about 1 mg of sample on 1 ml of sulphuric acid; it dissolves in the acid with an orange or brown-red colour.When this solution is diluted cautiously with water, the colour changes to brown, then to green, and finally to blue.12.Methylene blue dye (Colour Index No.52015)(i)Methylene blue dye shall be dark green powder as assessed by visual inspection and shall consist essentially of methylthionine chloride, C16H18CIN3S.(ii)Identification test. Mix 10 ml of a 0.01% solution with 1 ml of acetic acid and 100 mg of zinc powder and warm; the solution is decolourised. Filter and expose the filtrate to air; the blue colour returns.FOURTH SCHEDULE
TABLE FOR DETERMINING THE ORIGINAL GRAVITY OF WORTS
SpiritIndication | DegreesofOriginalGravity | SpiritIndication | DegreesofOriginalGravity | SpiritIndication | DegreesofOriginalGravity | SpiritIndication | DegreesofOriginalGravity |
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-0 | -00 | 4.1 | 17.75 | 8.2 | 36.58 | 12.3 | 56.38 |
-1 | -42 | 4.2 | 18.21 | 8.3 | 37.94 | 12.4 | 56.89 |
-2 | -85 | 4.3 | 18.66 | 8.4 | 37.51 | 12.5 | 57.40 |
-3 | 1.27 | 4.4 | 19.12 | 8.5 | 37.97 | 12.6 | 57.91 |
-4 | 1.70 | 4.5 | 19.57 | 8 .6 | 38.44 | 12.7 | 58.42 |
-5 | 2.12 | 4.6 | 20.03 | 8.7 | 38.90 | 12.8 | 58.93 |
-6 | 2.55 | 4.7 | 20.48 | 8.8 | 39.37 | 12.9 | 59.44 |
-7 | 2.97 | 4.8 | 20.94 | 8.9 | 39.83 | 13.0 | 59.95 |
-8 | 3.40 | 4.9 | 21.39 | 9.0 | 40.30 | 13.1 | 6.46 |
-9 | 3.82 | 5.0 | 21.85 | 9.1 | 40.77 | 13.2 | 60.97 |
1.0 | 4.25 | 5.1 | 22.30 | 9.2 | 41.24 | 13.3 | 61.48 |
1.1 | 4.67 | 5.2 | 22.76 | 9.3 | 41.71 | 13.4 | 61.99 |
1.2 | 5.10 | 5.3 | 23.21 | 9.4 | 42.18 | 13.5 | 62.51 |
1.3 | 5.52 | 5.4 | 23.67 | 9.5 | 42.65 | 13.6 | 63.01 |
1.4 | 5.95 | 5.5 | 24.12 | 9.6 | 43.12 | 13.7 | 63.52 |
1.3 | 5.52 | 5.4 | 23.67 | 9.5 | 42.65 | 13.8 | 64.03 |
1.4 | 5.95 | 5.5 | 24.12 | 9.6 | 43.12 | 13.9 | 64.54 |
1.5 | 6.37 | 5.6 | 24.58 | 9.7 | 43.59 | 14.0 | 65.10 |
1.6 | 6.80 | 5.7 | 25.03 | 9.8 | 44.06 | 14.1 | 65.62 |
1.7 | 7.22 | 5.8 | 25.49 | 9.9 | 44.53 | 14.2 | 66.14 |
1.8 | 7.65 | 4.9 | 25.94 | 10.0 | 45.00 | 14.3 | 66.66 |
1.9 | 8.07 | 6.0 | 26.40 | 10.1 | 45.48 | 14.4 | 67.18 |
2.0 | 8.50 | 6.1 | 26.86 | 10.2 | 45.97 | 14.5 | 67.70 |
2.1 | 8.94 | 6.2 | 27.32 | 10.3 | 46.45 | 14.6 | 68.22 |
2.2 | 9.38 | 6.3 | 27.78 | 10.4 | 46.94 | 14.7 | 68.74 |
2.3 | 9.82 | 6.4 | 28.24 | 10.5 | 47.42 | 14.8 | 69.26 |
2.4 | 10.26 | 6.5 | 28.70 | 10.6 | 47.91 | 14.9 | 69.78 |
2.5 | 10.70 | 6.6 | 29.16 | 10.7 | 48.39 | 15.0 | 70.30 |
2.6 | 11.14 | 6.7 | 29.62 | 10.8 | 48.88 | 15.1 | 70.83 |
2.7 | 11.58 | 6.8 | 30.08 | 10.9 | 49.36 | 15.2 | 71.36 |
2.8 | 12.02 | 6.9 | 30.54 | 11.0 | 49.85 | 15.3 | 71.89 |
2.9 | 12.46 | 7.0 | 31.00 | 11.1 | 50.35 | 15.4 | 72.42 |
3.0 | 12.90 | 7.1 | 31.46 | 11.2 | 50.85 | 15.5 | 72.95 |
3.1 | 13.34 | 7.2 | 31.93 | 11.3 | 51.35 | 15.6 | 73.48 |
3.2 | 13.78 | 7.3 | 32.39 | 11.4 | 51.85 | 15.7 | 74.01 |
3.3 | 14.22 | 7.4 | 32.86 | 11.5 | 52.35 | 15.8 | 74.54 |
3.4 | 14.66 | 7.5 | 33.32 | 11.6 | 52.85 | 15.9 | 75.07 |
3.5 | 15.10 | 7.6 | 33.79 | 11.7 | 53.35 | 16.0 | 75.60 |
3.6 | 15.54 | 7.7 | 34.25 | 11.8 | 53.85 | - | - |
3.7 | 15.98 | 7.8 | 34.72 | 11.9 | 54.35 | - | - |
3.8 | 16.42 | 7.9 | 35.18 | 12.0 | 54.85 | - | - |
4.0 | 17.30 | 8.1 | 36.11 | 12.2 | 55.87 | | |